罗科丽，陈丽仪，柯坚灿^*，卢 蔚，王乾蕾

（中山市食品药品检验所，广东中山 528400）

摘要：建立不完全快速消解石墨炉原子吸收测定婴幼儿食品中铅含量的快速检测方法，提升工作效率，减少环境污染。分别对消解试剂及用量、消解温度、消解时间进行优化，得出不完全快速消解石墨炉原子吸收光谱法的方案，并对方法进行验证和应用。结果表明，回收率在106%～137%之间，精密度在7%以内，准确度和精密度较好。该方法适用于铅含量较高的样品，可用于重金属污染等食品安全事件中铅含量的快速检测，可以为监管部门提供技术支持。

关键词：不完全快速消解；石墨炉原子吸收光谱法；婴幼儿食品；铅

中图分类号：TS207.3    文献标识码：A    文章编号：1674-506X（2023）02-0131-0004

Determination of Lead in Infant and Young Children Food by Incomplete Rapid Digestion Graphite Furnace Atomic Absorption Spectrometry

LUO Keli，CHEN Liyi，KE Jiancan*，LU Wei，WANG Qianlei

（Zhongshan Institute of Food and Drug Control, Zhongshan Guandong 528400, China）

Abstract：To establish a rapid method for the determination of lead in infant food by incomplete rapid digestion graphite furnace atomic absorption spectrometry, so as to improve work efficiency and reduce environmental pollution. The digestion reagent and dosage, digestion temperature and digestion time were optimized respectively, and the scheme of incomplete rapid digestion graphite furnace atomic absorption spectrometry was obtained, and the method was verified and applied. The results indicated that the recovery rate was between 106%～137%，and the precision was within 7%. The accuracy and precision were good. The method is suitable for samples with high lead content. It can be used for rapid detection of lead content in food safety events such as heavy metal pollution, and can provide technical support for regulatory authorities.

Keywords：incomplete rapid digestion; graphite furnace atomic absorption spectrometry; infant and young children food; lead

doi：10.3969/j.issn.1674-506X.2023.02-020

收稿日期：2022-05-16

基金项目：广东省市场监督管理局科技项目（项目编号：2021CS07）

作者简介：罗科丽（1985-），女，硕士，工程师。研究方向：食品安全检测。

*通信作者：柯坚灿（1989-），男，本科，工程师。研究方向：食品安全检测。

引用格式：罗科丽,陈丽仪,柯坚灿,等.不完全快速消解石墨炉原子吸收光谱法测定婴幼儿食品中铅含量[J].食品与发酵科技,2023,59(2):131-133,154.